Copper(II), nickel(II), palladium(II) and iron(III) complexes of 2-(3-phthalhydrazidylazo)-1,3-diketones
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چکیده
منابع مشابه
Preparation and Characterization of Ti(BH4)3(THF)3 and V(BH4)2(TMEDA)2 Complexes
We have recently synthesized Ti(BH4)3(THF)3 and V(BH4)2(TMEDA)2 complexes. The reaction of TiCl3(THF)3 with NaBH4 in dry THF gave flat blue crystals, Ti(BH4)3(THF)3. The reaction of VCl3 with NaBH4 in presence of N, N, N', N'- tetramethyle...
متن کاملpreparation and characterization of ti(bh4)3(thf)3 and v(bh4)2(tmeda)2 complexes
we have recently synthesized ti(bh4)3(thf)3 and v(bh4)2(tmeda)2 complexes. the reaction of ticl3(thf)3 with nabh4 in dry thf gave flat blue crystals, ti(bh4)3(thf)3. the reaction of vcl3 with nabh4 in presence of n, n, n', n'- tetramethylethylenediamine, tmeda, produced violet crystals, v(bh4)2(tmeda)2. vibrational and magnetic properties of ti(bh4)3(thf)3 and v(bh4)2(tmeda)2 have been studied.
متن کاملArylazo derivatives of some fluorinated β-diketones and their metal complexes
Phenylazo and benzothiazolylazo derivatives of trifluoroacetylacetone andhexafluoroacetylacetone have been synthesized and characterized. Analytical and spectral datarevealed the existence of phenylazo derivatives in the intramolecularly hydrogen-bonded ketohydrazoneform while the benzothiazolylazo derivatives in the azo-enol form. The monobasicbidentate coordination of the phenylazo derivative...
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The synthesis of SmCl3(THF)3 from SmCl3.6H2O is described. The reaction of SmCl3(THF)3 with NaBH4 in dry THF gave white microcrystalline tris (tetrahydroborato) tris (tetrahydrofuran) samarium (III), Sm(BH4)3(THF)3. The vibrational and magnetic properties of Sm(BH4)3...
متن کاملsynthesis and characterization of potentially biological active cyclometallated organoplatinum(ii) complexes
this work is presented in five parts. in the first part preparation of the starting complex [pt(c^n)cl(dmso)], 1, in which c^n = n(1),c(2?)-chelated, deprotonated 2-phenylpyridine, and dmso = dimethylsulfoxide, and its reaction with 1 equiv of the biphosphine ligands bis(diphenylphosphino)amine, dppa, or bis(diphenylphosphino)methane, dppm, to give the complex [pt(c^n)cl(dppa)], 2, or [pt(c^n)c...
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ژورنال
عنوان ژورنال: Journal of Chemical Sciences
سال: 1987
ISSN: 0253-4134,0973-7103
DOI: 10.1007/bf02900719